Crystal Structure of 2-Thiopyrrole-1,2-dicarboximide-(bis-triphenylphosphine)copper(I)chloride, [(Ph3P)2Cu(Cl)C6H4N2OS]

Krishna K. Pandey; Mathias Noltemeyer; In Memory: G.M. Sheldrick (1942–2025); Ray Saheb

doi:10.1515/znb-1984-0507

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In Memory: G.M. Sheldrick (1942–2025)

Crystal Structure of 2-Thiopyrrole-1,2-dicarboximide-(bis-triphenylphosphine)copper(I)chloride, [(Ph3P)2Cu(Cl)C6H4N2OS]

Zeitschrift für Naturforschung B 39(5): 586-589

Article 1984 English

Authors

KP
Krishna K. Pandey
MN
Mathias Noltemeyer
In Memory: G.M. Sheldrick (1942–2025)
University of Gottingen

Abstract

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Crystals of the title compound are monoclinic, space group C2/c, a = 3858.0(7), b = 1013.8(2), c = 2982.1(6) pm, β = 139.76(3)° and Z = 8. The structure was refined to R = 0.063 for 2155 unique observed diffractometer data. The copper atom is coordinated tetrahedrally by 2P, CI and S, contrary to a previous spectroscopic assignment

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Crystal Structure of 2-Thiopyrrole-1,2-dicarboximide-(bis-triphenylphosphine)copper(I)chloride, [(Ph<sub>3</sub>P)<sub>2</sub>Cu(Cl)C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>OS]

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