A new heterodinuclear cryptate [AgCuL](ClO4−)2 was synthesized by transmetallation via its precursor [Ag2L](ClO4−)2 (L = ligand). The electrospray mass spectrum (ES-MS) showed that the heterodinuclear entity exists in the solution. The X-Ray structure analysis shows that the AgI ion has tetrahedral geometry while CuI lies in a three-coordinate environment.
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