Reversible Addition-Fragmentation Chain Transfer Polymerization on different Synthesizer Platforms

Renzo M. Paulus; Martin W. M. Fijten; Mariska J. de la Mar; Richard Hoogenboom; Ulrich Sigmar Schubert

doi:10.1002/qsar.200520122

Abstract

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The reproducibility for different automated synthesizers was investigated on the basis of the reversible addition-fragmentation chain transfer (RAFT) polymerization of methyl methacrylate. Besides the reproducibility within one synthesizer and the comparability between different synthesizers also the effect of different reaction volumes (up-scaling) was investigated and compared to conventional lab experiment.

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