ChemInform Abstract: Synthesis and Characterization of Two‐Dimensional Nb4C3 (MXene).

Michael Ghidiu; Michael Naguib; Chenyang Shi; Olha Mashtalir; Long Pan; B. Zhang; Jian Yang; Yury Gogotsi; Simon J. L. Billinge; Michel W. Barsoum

doi:10.1002/chin.201440016

Abstract

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Abstract Phase‐pure, two‐dimensional Nb 4 C 3 T x (T x : general surface termination) is synthesized by immersion of Nb 4 AlC 3 powder (obtained by in situ hot pressing of mixtures of the elements at 3 MPa and 1700 °C for 1 h) in 48‐51% aqueous HF for 96 h at ambient temperature with stirring (77% yield).

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