ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTTitration of Isomeric Substituted 5-Amino-1,2,3-triazoles in Nonaqueous MediaEugene. Lieber, C. N. R. Rao, and T. S. ChaoCite this: Anal. Chem. 1957, 29, 6, 932–933Publication Date (Print):June 1, 1957Publication History Published online1 May 2002Published inissue 1 June 1957https://pubs.acs.org/doi/10.1021/ac60126a020https://doi.org/10.1021/ac60126a020research-articleACS PublicationsRequest reuse permissionsArticle Views62Altmetric-Citations4LEARN ABOUT THESE METRICSArticle Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. These metrics are regularly updated to reflect usage leading up to the last few days.Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Find more information about Crossref citation counts.The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Find more information on the Altmetric Attention Score and how the score is calculated. Share Add toView InAdd Full Text with ReferenceAdd Description ExportRISCitationCitation and abstractCitation and referencesMore Options Share onFacebookTwitterWechatLinked InRedditEmail Other access optionsGet e-Alertsclose Get e-Alerts
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
A new layered anionic zinc oxalate of the formula, K[C6N2H13][Zn2(C2O4)3].4H2O containing 12-membered honeycomb apertures has been synthesized hydrothermally in the presence of DABCO and K+. A noteworthy feature of the structure is the presence of 12-membered apertures, aligned in such a way as to create pseudo one-dimensional tunnels as in zeolitic structures. The amine, K+ and water molecules are present in the tunnels.
Magic nuclearity giant clusters formed by the mesoscale self-assembly of Pd nanocrystals of 2.5 nm diameter (nuclearity, ∼561) have been identified by transmission electron microscopy. The clusters have discrete diameters, corresponding to those expected for magic nuclearity of 13, 55, 147, 309, 561, and 1415 and corresponding to closed shells of 1, 2, 3, 4, 5, and 7, respectively. Imaging at different tilt angles has provided confirmation of the spherical nature of these giant clusters. Giant clusters of magic nuclearity have also been found with Pd nanocrystals of ∼3.2 nm diameter (nuclearity, ∼1415).
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
No abstract is provided for this article.
No abstract is provided for this article.
No abstract is provided for this article.
The electrochemical generation of green hydrogen as an alternative energy source requires higher energy inputs and suffers from low current output using non‐noble metal‐based catalysts. In this article, Nb3VS6 nanosheets have been utilized as catalysts to investigate the electrochemical hydrogen evolution reaction (HER) and the oxygen evolution reaction (OER) in an alkaline medium. Nb3VS6 nanosheets demonstrated considerable effectiveness as catalysts and strong activity, showing ampere‐level current densities and stability in the working potential range towards the electrochemical production of hydrogen. Nb3VS6 nanosheets exhibit a high current density of 1.5 A cm‐2 towards HER at an overpotential of 650 mV. Furthermore, its bifunctionality achieved an impressive current density of 1.8 A cm‐2 at a potential of 2.9 V in a full‐cell configuration.
